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1、behrS5fullyautomaticsteamdistillationapparatusbehrOperatingManualPleasereadthisoperatingmanualcarefullybeforestartinguseofyournewbehrS5steamdistillationapparatus!Theoperatingmanualprovidesclearandsimpleinstructionsintheuseoftheapparatus.Additionalinformation,whichisusefulandimportantforanunderstandi
2、ngoftheoperatingprinciplesoftheapparatus,isdenotedbyagraystripeinthemargin.AWewishyousuccessintheuseofthebehrS5SteamDistillationApparatusSafetyWarningsInordertoavoidelectricalshockinjury,pleaseinsurethatnoliquidsgetintotheapparatushousingAorcomeincontactwiththeelectricalwiresandconnections!AToavoide
3、lectricalshockinjury,alwaysremovetheelectricalpower(mainsplugbeforeopeningtheapparatushousing!ARepairofelectrical,electronicandmechanicalcomponentsisonlytobeperformedbysuitablyquali-?edandauthorizedpersonnel!APleaserigorouslyobserveallpertinentsafetymeasurestoavoidinjuryinworkingwithglass!AObserveca
4、refullysafetyproceduresinworkingwithacidsandbases,whichcancauseburnsandotherinjuries!ADuringthedistillationandforashorttimethereafter,donottouchanypartsofthedistillationsystembehindthePlexiglasdoor!Thesecomponentsmaybehotandcancauseburninjury!DonotoperatetheS5steamdistillationapparatusindamporexplos
5、iveatmospheres!AThemaximumallowablehumidityis80%ThemaximumallowableroomtemperatureiS50C0BeforeshuttingtheS5down22Insertingthevessels22Switchingthesteamdistillationapparatuson22Rinsing22Purgingprogram23AdaptingthebehrS5toyourpersonalrequirements24Choosingthelanguage24Con?gurngthelevelsensor24Settirth
6、etime24DownloadSoftware-Updates24selectingtitrationunit24CoolingWaterSourceSetting24Whattodoif(25Problemswhichyoucansolveyourself25Samplevesselnotinserted25Insuf?cientcoolingwaterpressure25Reagentlevelsensors25IntheeventthatyouarenotusingthebehrKAS50canisterset:25IntheeventthatyouareusingthebehrKAS5
7、0canisterset:25Titrationvesselisfull26Problemsrequiringtheattentionofthebehrrepairservice27TechnicalSpeci?cations28Overwiew:MenusanddisplaysofthebehrS529TableofContentsContentsofDelivery5UseofthebehrS5inChemicalAnalyses5OperatingConditions5InstallingthebehrS57Emplacingthesteamdistillationapparatus7C
8、onnectingthehosesandtubing8Connectingtotheelectricalpowerline8FrontviewofthebehrS511Turningthesteamdistillationapparatuson12Preparations12SwitchingtheS5on12DistillingwiththebehrS513Theoperatingcontrolunit13ProgrammingtheS513Distilling16(Re?llingthereagentlines16Insertingtheglasscomponents16Switching
9、thesteamdistillationapparatuson16Performingthe(re?llng17Testrun17Insertingtheglassvessels17Switchingthesteamdistillationapparatuson17Startingthetestrun18Endingthetestrun18AutomaticDistillationwiththebehrS519Insertingthevessels19Switchingthesteamdistillationapparatuson19Startingtheautomaticdistillati
10、on19Interruptingorterminatingthedistillationprogram19Endingtheautomaticdistillation19ManualdistillationwiththebehrS520Insertingthesamplevessel20Switchingthesteamdistillationapparatuson20Performingamanualdistillation20Endingthemanualdistillation21ContentsofDeliveryPleasecheckimmediatelyuponreceipttos
11、eethatthecontentsofdeliveryarecompleteandundamaged.Intheeventofdamageinshipment,contacttheship-pingagent(mail,freightcarrier,railwayimmediatelyandrequestaninspectionofactualconditionofcontentsandpackaging.Thecomponents,whichshouldbepresent,areitemizedinthefollowinglist.ListofComponentsbehrS5distilla
12、tionapparatus,completelyassembledHoseset:1 Water inlet hose, 10/17, withandstandard ? ttings,2m1Verprenetubing,8/12,2m3PVCtubing,4/7,2m2PVCtubing,8/12,2m3PVCtube,6x1,420mm1PVCtube,10x1,420mm1Electrical(mainscable1Cablefortitratorconnection1CableforpHelectrode1CrucibletongsUseofthebehrS5inChemicalAna
13、lysesThebehrS5isaneffectiveautomaticdistillationappa-ratusforuseinvariousapplications.Principally,it?ndsapplicationinthesteamdistillationofKjeldahlammoniasolutions.Inthisapplication,theautomaticadditionofNaOH,HOandH3BO3,aswellastheautomaticdrain-ingofspentsamplewaste,provideforahighdegreeofsafetyand
14、convenienceinuse.Becertaintocarefullyimplementthefollowingguidanceforthesakeofsafetyinoperationandthegreatestpos-sibleworkinglifeofthebehrS5:Operatetheapparatusalwaysinaccordancewiththeinstructionsandwarningsinthisoperatingmanual!Modi?cationorchangestotheapparatusareunauthorizedandleadtoterminationo
15、ftheguaiantee.Modi?cationsmayresultinseriousopera-tionalsafetyhazardsand/orreducedreliabilityoftheS5.Donotexposethesteamdistillationunittocor-rosivevapors,suchasacids,basesororganicsolvents!OperatingConditionsOperatethebehrS5steamdistillationapparatusun-dernormallaboratoryconditions.TheS5steamdistillationapparatusmaybecon-nectedtoacoldwatertaphavingastandard?pipethread.ContentsofDelivery-5-?behrLabor-Technik20061.21.31.41.51.61.71.81.91.111.141.151.161.101.131.12Figure.1:behrS5-rearviewRearviewofthebehrS5Figure1:DiagramLegend1.1Overpressuresteamreleas
