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1、中药中药中药中药红外光谱分析与鉴定红外光谱分析与鉴定红外光谱分析与鉴定红外光谱分析与鉴定药材药材药材药材/ / / /饮片饮片饮片饮片孙素琴孙素琴孙素琴孙素琴清华大学化学系清华大学化学系清华大学化学系清华大学化学系中药红外光谱中药红外光谱质量控制：全过程质量控制：全过程炮制炮制提取提取中药红外光谱中药红外光谱质量控制：多层次质量控制：多层次全部成分，指纹图谱全部成分，指纹图谱全部成分，指纹图谱全部成分，指纹图谱特定成分，定性定量特定成分，定性定量特定成分，定性定量特定成分，定性定量主体成分分析主体成分分析油脂油脂4000.03000200015001000400.0 cm-1A 3301301
2、0292728551746 165615411461139812401162 1101 999723 597330130082926285517471656 15441460 1239116211001056789721588331830092925 2854 174616581545 145712401159 10981055 787722 618336030072926285517451522137812301056895 782596火麻仁火麻仁芥子芥子莱菔子莱菔子乌梅乌梅 Wavenumbers / cm-1Absorbance主体成分分析主体成分分析油脂油脂火麻仁火麻仁芥子芥子莱菔子
3、莱菔子乌梅乌梅 285417473100.0300029002800.0 cm-1A 3010295929262895 287328543009295929252894 287328543009295929242873285430082958292528731800.017001600150014001300.0 cm-1A 174617111658151314671441 14161379174616571546151214671440137817471711 165715491515146717201657151714672nd derivative/Wavenumbers / cm-1/
4、主体成分分析主体成分分析油脂油脂芥子芥子乌梅乌梅 火麻仁火麻仁莱菔子莱菔子主体成分分析主体成分分析蛋白质蛋白质4000.03000200015001000400.0 cm-1A 331330742960 2933287516581525145213951308124010766213282308229222851164915421451132412401041615573330129582927287428551659154314531400131112371156107910446233354292616481545138012391071892615527羚羊角羚羊角麝香麝香水蛭水蛭相思子
5、相思子Wavenumbers / cm-1Absorbance主体成分分析主体成分分析蛋白质蛋白质1800.017001600150014001300.0 cm-1A 1659 1640162815661511 14991452138717451696 166016271566 1514150014691440 136713241692 164015661548 15151500 1468 1453140217461550 1511149914691639Wavenumbers / cm-12nd derivative羚羊角羚羊角麝香麝香水蛭水蛭相思子相思子主体成分分析主体成分分析蛋白质蛋白质
6、麝香麝香相思子相思子羚羊角羚羊角水蛭水蛭主体成分分析主体成分分析淀粉淀粉4000.03000200015001000400.0 cm-1A 33732929 16601537146213791240116110811015995932861762709573528339129301642151614181372124311581080101593286176771057552833622928 1656145714181371 124511591080994931862765709575528333429341653146014211369124111591083991928862768709
7、575532白果白果干姜干姜甘遂甘遂山药山药 Wavenumbers / cm-1Absorbance4000.03000200015001000400.00.000.10.20.30.40.50.60.70.80.91.01.10cm-1A 339129301650 1461141913711242115910811015995927859764709574528淀粉淀粉主体成分分析主体成分分析淀粉淀粉1500.0140012001000800600500.0 cm-1A 1168108398892686357411671079983922 863767 574146811631078 98
8、9921862574146911621078985920767572白果白果干姜干姜甘遂甘遂山药山药 862Wavenumbers / cm-12nd derivative1500.0140012001000800600500.0-0.00300-0.0025-0.0020-0.0015-0.0010-0.00050.00000.00050.00100.00150.00200.00250.00300cm-1A 1469120811621108107810581016985922 861764710613572529淀粉淀粉主体成分分析主体成分分析淀粉淀粉白果白果甘遂甘遂干姜干姜山药山药 主体成
9、分分析主体成分分析蔗糖蔗糖4000.03000200015001000400.0 cm-1A 339229141733163614301375124210681053991921867588333929282856 1745165615471439124010691052 1015 991921867579356333893338294116531430134712791240111610681013 990909867 84968158355133892932 173616221430 124110681051 1014991920866577Wavenumbers / cm-1Absorb
10、ance4000.03000200015001000400.00.000.10.20.30.40.50.60.70.80.91.01.10cm-1A 472551583 682 7328498689099911013105310701129120812391279134614301460163129132942333833903562蔗糖蔗糖 白茅根白茅根川芎川芎当归当归独活独活主体成分分析主体成分分析蔗糖蔗糖1200.01150110010501000950900850800.0 cm-1A 1162110410691052989942 921 90886711611069105210149
11、89942 921 90886711721139 110410681052 10371014989942 921 90886784911611069 10521014941 9219088671200.01150110010501000950900850800.0-0.0200-0.015-0.010-0.0050.0000.0050.0100.0150cm-1A 8498688879099219429901004101410381053107010861104111611381161 1171蔗糖蔗糖Wavenumbers / cm-12nd derivative白茅根白茅根川芎川芎当归当归
12、独活独活主体成分分析主体成分分析蔗糖蔗糖白茅根白茅根当归当归川芎川芎独活独活主体成分分析主体成分分析水苏糖水苏糖4000.03000200015001000400.0 cm-1A 33912926164914111351 114310621028993 873799687335229311635 1412 126511451055872798 33922926 16321423136011441048 9968717973391293016471420 135411431051871797Wavenumbers / cm-1Absorbance水苏糖水苏糖丹参丹参地黄地黄玄参玄参主体成分分析主
13、体成分分析水苏糖水苏糖1200.011001000900800700.0 cm-1A 11601081 1028988923871831 80077411611112107999791787179976611621107 107898391987083279976911071079987921869 8328007691162水苏糖水苏糖丹参丹参地黄地黄玄参玄参Wavenumbers / cm-12nd derivative主体成分分析主体成分分析鞣质鞣质4000.03000200015001000400.0 cm-1A 3384 2927171416471615151314491337 12
14、3110581035832755602336529361728161515091445133612261042876749 6033352292817141613153514481322120010801026870757 64958733441720161415171447133312101036875757 604Wavenumbers / cm-1Absorbance诃子诃子石榴皮石榴皮五倍子五倍子藏青果藏青果主体成分分析主体成分分析鞣质鞣质1800.0170016001500140013001200.0 cm-1A 1685164816181511145313881294 1276 1
15、23717471619151014411316 12301729 16121548153615121470144213121788 17001688165415111470 14471337Wavenumbers / cm-12nd derivative诃子诃子石榴皮石榴皮五倍子五倍子藏青果藏青果特定成分分析特定成分分析草酸盐草酸盐4000.03000200015001000400.0 cm-1A 34303348 2929161914241317 11541022 780666 517342933393068293216201449131611501027781 6645163348292228521642131810747816225363351 292528531732162514471318107078165961551634883339 306116181318884782 662516Wavenumbers / cm-1Absorbance白鲜皮白鲜皮地骨皮地骨皮桑叶桑叶银杏叶银杏叶草酸钙草酸钙特定成分分析特定成分分析草酸盐草酸盐白鲜皮白鲜皮地骨皮地骨皮桑叶桑叶银杏叶银杏叶草酸钙草酸钙1800.01600140012001000
