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1、California Environmental Protection Agency Air Resources Board METHOD 310 DETERMINATION OF VOLATILE ORGANIC COMPOUNDS VOC IN CONSUMER PRODUCTS AND REACTIVE ORGANIC COMPOUNDS IN AEROSOL COATING PRODUCTS Including Appendices A and B Adopted September 25 1997 Amended September 3 1999 Amended June 22 20
2、001 DISCLAIMER Mention of any trade name or commercial product in Method 31 0 does not constitute endorsement or recommendation of this product by the Air Resources Board METHOD 310 DETERMINATION OF VOLATILE ORGANIC COMPOUNDS VOC IN CONSUMER PRODUCTS AND REACTIVE ORGANIC COMPOUNDS IN AEROSOL COATING
3、 PRODUCTS 1 APPLICABILITY 1 I This method Method 310 applies to the determination of the percent by weight of 1 volatile organic compounds VOC in consumer products antiperspirant and deodorant products and aerosol coatings products as those terms are defined in Title 17 California Code of Regulation
4、s CCR Division 3 Chapter 1 Subchapter 8 5 Consumer Products commencing with section 94500 and 2 low vapor pressure volatile organic compounds LVP VOC as that term is defined in section 94508 a 78 and 3 the reactive organic compounds ROC contained in aerosol coating products as that term is defined i
5、n Title 17 CCR section 94521 Method 310 determines the total volatile material in a product and the presence of any compounds prohibited by ARB regulations prohibited compounds Components of the product that do not meet the definition of a VOC or are exempted by ARB regulations for a specific produc
6、t category exempt compounds are subtracted from the total volatile material to determine the final VOC content for the product Method 310 is also used to determine the percent by weight of the ROCs contained in aerosol coating products for the purpose of determining compliance with the Regulation fo
7、r Reducing the Ozone Formed from Aerosol Coating Product Emissions Title 17 CCR sections 94520 to 94528 the Aerosol Coatings Regulation 1 3 Method 310 does not apply to the determination of the composition or concentration of fragrance components in products 1 4 The term Executive Officer as used in
8、 this document means the Executive Officer of the Air Resources Board or his or her authorized representative 2 TEST METHODS Method 310 incorporates by reference the following American Society for Testing and Materials ASTM National Institute for Occupational Safety and Health NIOSH and United State
9、s Environmental Protection Agency US EPA analytical test methods ASTM D 2369 97 Standard Test Method for Volatile Content of Coatings July 10 1997 ASTM D 1426 93 Standard Test Methods for Ammonia Nitrogen in Water September 15 1993 ASTM D 4017 96a Standard Test Method for Water in Paints and Paint M
10、aterials by the Karl Fisher Titration Method July 10 1996 ASTM D 3792 91 Standard Test Method for Water Content of Water Reducible Paints by Direct Injection Into a Gas Chromatograph May 15 1991 ASTM D 859 94 Standard Test Method for Silica in Water determination of polymethylsiloxanes after digesti
11、on May 15 1994 ASTM D 3074 94 Standard Test Methods for Pressure in Metal Aerosol Containers November 15 1994 with the modifications found in Appendix A to this Method 31 0 ASTM D 3063 94 Standard Test Methods for Pressure in Glass Aerosol Bottles November 15 1994 with the modifications found in App
12、endix A to this Method 31 0 ASTM D 3064 89 Standard Terminology Relating to Aerosol Products November 24 1989 NIOSH Method 1400 Alcohols I analysis of acetone and ethanol by gas chromatography NIOSH Manual of Analytical Methods Volume 1 February 1 984 Gas ChromatographylMass Spectrometry for Volatil
13、e Organics analysis of exempt and prohibited compounds in the product by headspacelgas chromatographylmass spectrometry 2 10 1 US EPA Method 8240B September 1994 Revision 2 Volatile Organic Compounds by Gas ChromatographylMass Spectrometry GCIMS Test Methods for Evaluating Solid Waste Volume 1 B Cha
14、pter 4 Section 4 3 2 Laboratory Manual PhysicalIChemical Methods SW 846 September 1994 2 10 2 US EPA Method 8260B December 1996 Revision 2 Volatile Organic Compounds by Gas ChromatographylMass Spectrometry GCIMS Test Methods for Evaluating Solid Waste Volume 1 B Chapter 4 Section 4 3 2 Laboratory Ma
15、nual PhysicalIChemical Methods SW 846 December 1996 US EPA Reference Method 24 Determination of Volatile Matter Content Water Content Density Volume Solids and Weight Solids of Surface Coatings 40 Code of Federal Regulations CFR Part 60 Appendix A as it existed on July 1 1994 US EPA Reference Method
16、 24A Determination of Volatile Matter Content and Density of Printing Inks and Related Coatings 40 CFR Part 60 Appendix A as it existed on July 1 1994 US EPA Reference Method 18 Measurement of Gaseous Organic Compound Emissions by Gas Chromatography 40 CFR Part 60 Appendix A as it existed on July 1 1994 US EPA Method 300 7 March 1986 Dissolved Sodium Ammonium Potassium and Calcium in Wet Deposition by Chemically Suppressed Ion Chromatography ASTM D 86 96 Standard Test Methods for Distillation of