常见溶剂旳化学位移常见溶剂旳１Ｈ在不同氘代溶剂中旳化学位移值 mｕlt.氘 代 溶 剂CDＣｌ3(CD３)2CＯ(CD3)２SOC６D6CD３CNCD3ＯDD２OC５Ｄ5N残存溶剂峰 7.2６2.052.５07.161.943．314.7９７．2０7．５78.72水峰brs1.562.8４３.330.4０2．134.874.79４.９6ＣＨCl３ｓ7.２68.028．3２6．１５7．587．9０ (CH3)2CＯs２．172.09２.091.5５2.0８2.１5２．22(CH３)２SOs2.622．５22.541.682．502．６52．71Ｃ6Ｈ6s７.３６7.367.377.157.37７.33 CH3ＣNs２.102.０５2.071.551.962．03２.06CH3ＯHＣＨ3,sﻫＯH,ｓ３.4９１．０93．31ﻫ3.１2３.164.０13.073.282.163.３4３.３4C5Ｈ5ＮCH（2），ｍCH(3），mﻫCH(4),m ８．62ﻫ7．２9ﻫ7.６8８.5８7.35ﻫ7.768.5８ﻫ７．３9ﻫ７.798.53ﻫ６.66ﻫ6．９88.57ﻫ7．３3ﻫ7.７38.53ﻫ7.447.858．5２ﻫ7．45ﻫ7．878.72ﻫ7．２0ﻫ7.57CH3CＯOC2H5CH3,ｓCH２，qCH3,t2.０54.１2ﻫ1.261.974．05ﻫ1.20１.９9ﻫ4.031.171．６53.8９ﻫ0.９21．９7ﻫ4.0６ﻫ1．２０2.０14.0９ﻫ１.24２．074.14ﻫ1.24CＨ2Ｃl2s５.305.6３5.７６4.２7５.4４5.４9ｎ-ｈｅxaneCH3,ｔﻫCH2,m0.88ﻫ1.260．８81．280．861.250．８9ﻫ1.240.8９1.280．90１.2９Ｃ2H5OHCH3,tﻫＣH２,ｑ1.2５ﻫ3.７２１.1２ﻫ3.５71.０6ﻫ3.4４０.963.3４1.123.541.193.601．1７ﻫ３.6５常见溶剂旳化学位移常见溶剂旳13C在不同氘代溶剂中旳化学位移值 氘 代 溶 剂CDＣl３(ＣD3）2ＣO(CD3)2SＯＣ6D６ＣD3CNCD3ODＤ2OC5D5N溶剂峰77.16206．２629.８439.521２８.０６1.３211８.264９．00－123.４４135.43149．84CHCl377.３67９.１９７9．１677.7979.177９．44(CＨ3)2CO２07．0７30.9２２０5.8７３0.６020６．3130.５6204.４33０.１4２０７.433０.91２０９.67３0．６７21５.9430.89(ＣH3)２SＯ40．7641.2３40.4５40.0341.３1４0.4５3９．39C6Ｈ6128.37１2９.15１２8.3０12８．６2１29.32１２９.3４CH3ＣＮ１1６.431．891１7．６０ﻫ1.12117.91ﻫ1.031１6．０２０.２0１1８．26ﻫ1．7９11８.０6ﻫ0.85１19.68ﻫ1．４7CH3ＯH50．4１4９.774８.59４9．９７49.9０49.８６49．５0C5H５Ｎ149.９0１2３.7５ﻫ135.96１５0.67ﻫ12４．57ﻫ136.56１49.５８12３.８41３6.０５1５０．27ﻫ１2３.58ﻫ1３5.28１50.76ﻫ127.76ﻫ13６.8９１５0.０7ﻫ１25.５3１38.35149.１81２5．12138.27ＣH3ＣOOC2H5２1．0４１７1.3660.４914.1９２０.8３ﻫ１70.9６ﻫ６0.５614.5０２０.68170.３159.74ﻫ１4.4０20.５6170.4460.2114.19２１.16ﻫ171.6860.981４．54２0.８8ﻫ17２．8９ﻫ61.5014.49２1.1５17５.２６ﻫ62.3213.９2CH2Cl253．5254.9554.８４5３.465５.3２54.78ｎ-heｘane14．1４ﻫ22.7031．6414.3４２3.2832．3013．88ﻫ２2．０53０.9５１4.32ﻫ2３.0431.9614.4323.４032.3614.45２3.6832.73。