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1、工业结晶过程,主讲教师：杨亦文 工学博士/教授，博导 浙江大学化工系制药工程研究所 E-mail: Tel: 13588738628(538628) 2012.11,工业结晶过程 Industrial Crystallization,一、工业结晶概论 Chapter 1 Overview of Industrial Crystallization 结晶在工业上的应用 Utilization of Crystallization in Industries 结晶产品的表征 Characterization of Crystalline Products 溶解度和过饱和度 Solubility
2、and Supersaturation,工业结晶过程 Industrial Crystallization,二、成核 Chapter 2 Nucleation 初级成核 Primary Nucleation 二次成核 Secondary Nucleation 工业结晶器中的成核 Nucleation in Industrial Crystallizers,工业结晶过程 Industrial Crystallization,三、晶体生长 Chapter 3 Crystal Growth 晶体生长过程 Process Involved in Growth of Crystals 总的晶体生长过程
3、The Overall Crystal Growth Process 总的晶体生长动力学 The Overall Growth Kinetics 生长弥散 Growth Dispersion,工业结晶过程 Industrial Crystallization,四、粒数衡算概念 Chapter 4 Population Balance Concept 结晶系统数学模型 Mathematical Model of Crystallization systems 粒数衡算 Population Balance 通用粒数方程 The General Population Equation 分布矩 Mo
4、ments of The Distribution 平均粒度 Average Sizes 变异系数 Coefficient of Variation,工业结晶过程 Industrial Crystallization,五、混合悬浮混合产品取出结晶器：一种理想方式 Chapter 5 Mixed Suspension Mixed Product Removal Crystallizer-An Idealized Configuration 混合悬浮混合产品取出概念 Mixed Suspension Mixed Product Removal Crystallizer Concept MSMPR方
5、式的粒数衡算 Population Balance for The MSMPR Configuration MSMPR结晶器的粒数密度分布当晶体生长速度与粒径无关时 Population Density Distribution for MSMPR CrystallizerSize Independent Crystal Growth Rate MSMPR结晶器的粒数密度分布当晶体生长速度与粒径有关时 Population Density Distribution for MSMPR CrystallizerSize Dependent Crystal Growth Rate,工业结晶过程 I
6、ndustrial Crystallization,六、粒数影响因素 Chapter 6 Population Functions 与MSMPR结晶方式的偏差 Deviations from The MSMPR Crystallizer Configuration 分级 Classification,工业结晶过程 Industrial Crystallization,七、结晶动力学的求取 Chapter 7 Derivation of Crystallization Kinetics 纯粹结晶动力学的求取 Derivation of Pure Crystallization Kinetics
7、就外推得到的粒数密度数据的解释 Interpretation Population Density Data Obtained Resorting to Extrapolation 受粒数函数影响的结晶动力学的求取 Derivation of Crystallization Kinetics from Distributions Affected by Population Functions,工业结晶过程 Industrial Crystallization,八、结晶过程中的物理传递现象 Chapter 8 Physical Transport Phenomena in Crystalliz
8、ation 均相液体的混合 Mixing of Homogeneous Liquids 固液悬浮物的混合 Mixing of Solid/Liquid Suspensions 固液悬浮物中的传质 Mass Transfer in Solid/Liquid Suspensions 搅拌槽中的传热 Heat Transfer in Agitated Vessels,工业结晶过程 Industrial Crystallization,九、结晶系统的取样和分析 Chapter 9 Sampling and Analyzing Crystallizing Systems 液相样品的取样和分析 Sampl
9、ing and Analyzing Liquid Phase Samples 固相样品的取样和分析 Sampling and Analyzing Solid Phase Samples,工业结晶过程 Industrial Crystallization,十、结晶器设计中基本原理的应用 Chapter 10 The Use of Fundamental Principles in Crystallizer Design 1、物料衡算用于确定结晶器体积 The Use of Mass Balance to Formulate Crystallization Volume 2、粒数衡算概念用于表征产
10、品晶体粒度分布 The Use of The Population Balance Concept to Characterize Product Crystal Size Distributions 3、工业结晶器中结晶动力学与操作条件的相互作用 Interactions Between Crystallization Kinetics and Operation Conditions in Industrial Crystallizers 4、工业结晶过程中的技术问题 Technical Problems in Industrial Crystallization,工业结晶过程 Indus
11、trial Crystallization,十一、面向设计的结晶动力学：从小型实验取得的结晶动力学在结晶器设计上的应用 Chapter 11 Design Oriented Crystallization Kinetics Obtained in Small Scale Experiments for Crystallization Design 1、取得面向设计的结晶动力学的标准过程 Standardized procedure to derive design oriented crystallization kinetics 2、标准结晶动力学在结晶器设计中的应用 The Use of
12、Standard Crystallization Kinetics in Crystallizer Design 从小型实验取得的结晶动力学用于大型结晶器设计 The Use of Crystallization Kinetics Obtained in Small Scale Experiments for Design of Large Crystallizers,工业结晶过程 Industrial Crystallization,十二、间歇结晶器设计 Chapter 12 Design of Batch Crystallizers 间歇结晶操作的概念 Concept of Operati
13、on in Batch Crystallization 间歇结晶的一个循环 Description of A Cycle in Batch Crystallization 间歇过程的结晶周期 Description of A Crystallization Period in A Batch Cycle 间歇与连续操作的比较 Comparison of Batch and Continuous Operation 不稳定粒数衡算 The Unsteady State Number Balance 加晶种间歇结晶器设计：能量传递的最佳控制 Design of Seeded Batch Cryst
14、allizers Featuring on Optimal Control of Energy Transfer,工业结晶过程 Industrial Crystallization,十三、连续搅拌槽式结晶器设计 Chapter 13 Design of Continuous Stirred Tank Crystallizer 混合产品取出的连续全混结晶器的设计 Design of Continuous Well Mixed Crystallizers with Mixed Product Removal 强制内循环连续蒸发结晶器设计 Design of Continuous Evaporati
15、ve Crystallizers with Forced Internal Circulation 细晶消除的全混结晶器设计 Design of Well-Mixed Crystallizers with Fines Removal 分级产品取出的全混结晶器设计 Design of Well-Mixed Crystallizers with Classified Product Removal 同时消除细晶和分级产品取出的全混结晶器设计 Design of Well-Mixed Crystallizers with Simultaneously Operative Fines Destruct
16、ion and Classified Product Removal,工业结晶过程 Industrial Crystallization,十四、强制循环蒸发结晶器设计 Chapter 14 Design of Forced Circulation Evaporative Crystallizer 引言与工作原理 Introduction and Principles of Operation 蒸发结晶衡算 Balances in Evaporative Crystallization 固体分级 Solids Classification 与粒径有关的晶体生长速率 Size Dependent Growth Rates 浓度推动力分布 Distribution of Concentration Driving Force 液相流动模型 Liquid Phase Flow Model 推动力衡算 Driving Force Balances 区域停留时间 Sectional Residence Times 拟粒径有关
